Thermogravimetric analysis or thermal gravimetric analysis (TGA) is a method in which the mass of a sample is measured over time as the temperature changes. This measurement provides information about physical phenomena such as mass changes, temperature stability., oxidation/reduction behaviuor, decomposition, corrosion studies, compositional analysis and thermokinetics
A typical thermogravimetric analyzer consists of a precision balance with a sample pan located inside a furnace with temperature. The temperature is generally increased at a constant rate. The thermal reaction may occur under various atmospheres e.g. air, vacuum, inert gas, oxidizing/reducing gases, corrosive gases etc. Pressure may also be varied, e.g. high vacuum, high pressure, constant pressure, or controlled pressure.
TGA is a useful technique for studying polymeric materials, including thermoplastics, thermosets, elastomers, composites, plastic films, fibers, coatings, paints, and fuels.
Temperature range -150°C to 2400°
Heating rate 0.001 to 50 K/min
Sensors TGA, TGA-DTA, TGA-DSC, TGA-DSCcp
Vacuum-tight 10-4 mbar
Atmospheres Inert, oxidizing, static, dynamic, vacuum
Temperature resolution 0.001 K
Balance resolution 0.1 μg (over the entire weighing range)
Maximum sample load 35000 mg (incl. crucible), DSC: 0.19 ml, DTA: 0.9 ml
DSC enthalpy accuracy ± 2% (for most materials)
In house: TGA/DSC - MS Netzsch STA 449 FS QMS 403 C